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高温电热法制备高致密魔芋海绵

Highly Porous KGM Sponge by an Electrothermic Process at High Temperature

  • 摘要: 以魔芋纯化粉为原料,采用高温电热法制备高致密魔芋海绵,研究了电热条件及加热工艺对魔芋海绵结构和力学性能的影响。采用傅里叶红外光谱、光学显微镜和拉力仪对魔芋海绵的官能团、形貌结构和力学性能进行了表征。结果表明:魔芋6 g,发泡剂N,N-二亚硝基五亚甲基四胺0.6 g,加热温度220℃,电热时间35 min时,可制备孔隙率为72.69%的高致密魔芋海绵,其表观密度为0.256 9 g/cm3,内部呈三维网状结构,红外结果显示其主要成分是脱乙酰基魔芋葡甘聚糖(d-KGM),平均拉伸强度达到0.047 3 N/cm3,断裂伸长率达到283.6%。

     

    Abstract: Highly porous konjac-glucomannan(KGM) sponges were fabricated by an electrothermic process at high temperature. Influences of electrothermic conditions and heating modes on KGM sponge's structural and mechanical properties were invesgated. Fourier transform infrared spectrum, optical microscope and tension meter were used to measure KGM sponge's functional groups, morphology structure and mechanical properties. The results showed that the optimum condition was as follows:heating 35 min at 220℃ could obtain the products with the porosity and density of 72.69% and 0.2569 g/cm3 respectively. The microscopic image of KGM sponge showed a three-dimensional (3D) network, and the main component of it was deacetyl konjac glucomannan (d-KGM). The average tensile strength and elongation at break were 0.0473 N/cm3 and 283.6%.

     

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