麦草低温氧碱蒸煮黑液降黏技术
Viscosity Reduction Technology of Wheat Straw Alkaline-oxygen Pulping Black Liquor at Low Temperature
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摘要: 麦草经碱法蒸煮后,所得浆料不经洗涤,直接通入氧气进行处理。以黑液黏度,浆料卡伯值为考核指标,设置4因素3水平正交试验,对试验结果作极差分析发现,在用碱量0~2 %、氧压0.2~0.6 MPa、温度70~100 ℃和时间30~90 min 内得到较适宜的工艺条件为:用碱量 1 %,氧压 0.6 MPa,温度 85 ℃,时间 60 min。氧碱蒸煮结果为:黑液黏度 3.4 mPa·s,浆料卡伯值17.9。与第一段碱法蒸煮相比,黑液黏度降低 33.3 %,浆料卡伯值降低 11.8 %。Abstract: The wheat straw fibers after alkaline-AQ pulping was handled by oxygen directly without washing in present study. A L9(34) orthogonal design, including the factors of alkali charge, oxygen dosage, cooking temperature and holding time, was applied to evaluate their influences on black liquor viscosity and pulp Kappa number. The high quality pulp fibers with black viscosity 3.4 mPa·s and Kappa number 17.9 was obtained when the unwashed fibers were treated by 1% alkali charge (as NaOH) and 0.6 MPa oxygen pressure for 60 minutes at 85 ℃. In contrast to the pulp after first stage alkaline pulping, the black liquor viscosity and Kappa number decreased 33.3% and 11.8%, respectively.